Physical Review Volume 53, page 318.
Not paywalled as of 2024! A miracle! It is barely one page long.
This is the paper that contains the first successful report of experimental nuclear magnetic moment observation.
They promise more at the end:and this promise was fulfilled on the later The Molecular Beam Resonance Method for Measuring Nuclear Magnetic Moments.
We have tried this experiment with LiC1 and observed the resonance peaks of Li and Cl. The effects are very striking and the resonances sharp (Fig. 1). A full account of this experiment, together with the values of the nuclear moments, will be published when the homogeneous field is recalibrated.
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