Fix an effective numbering of Turing machines and use the diagonal halting set
It is computably enumerable: dovetail all the computations and output each index when its computation halts. It is not a recursive set. Otherwise a machine could, on input , loop if the alleged decider says and halt otherwise. Applying this machine to its own index contradicts either answer. Hence is computably enumerable but not a recursive set.
With the diagonal halting set , define
If were computably enumerable, its odd-index inverse image would make computably enumerable. If were computably enumerable, its even-index inverse image would do the same. But a set and its complement being computably enumerable would make the set a recursive set: run the two enumerations in parallel until the input appears in one. This contradicts the undecidability of . Thus neither nor its complement is computably enumerable.

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