A reference-sensitivity cancellation check determines whether a proposed comparison really removes the influence of a shared calibration reference. It checks the measurand, the reference's sensitivity coefficients and the range over which the claimed cancellation applies.
For estimates and , a contrast has local reference sensitivity
Its first-order reference variance is . Checking the contrast directly and checking the full covariance propagation should agree. The GUM defines the sensitivities and retains correlations between inputs.[ref]
An original linear model is and . For , the sensitivity is . Recomputing the unchanged comparison with the assigned reference value increased by changes by . With reference standard uncertainty 20 nm, its contribution to this contrast is 0.4 nm. Treating the two uses of as independent would miss this suppression.
A useful computational check perturbs one shared input consistently in every place it occurs. Perturbing its occurrences independently tests a different model. Finite-perturbation reference sensitivity also reveals whether a derivative evaluated at one point adequately describes the actual uncertainty range.
Zero first derivative is weaker than exact invariance. For an illustrative nonlinear model, take and . The derivative of vanishes at , but a reference perturbation leaves a term . If is zero-mean normal with standard deviation , that term has mean and standard deviation . The first-order cancellation has not removed the nonlinear contribution.
With stipulated and , these are nm and about 1.41 nm. These are model coefficients, not measured comparator behaviour.
Finally, verify that the chosen contrast is the quantity the experiment intends to determine. Replacing by another combination solely to cancel a reference changes the question. Retain calibration lineage and independent checks on comparator response; NIST's physical uncertainty budget distinguishes the master history from comparison-process variability.[ref]
Step-size stability of a reference perturbation checks whether a numerical reference-response estimate behaves consistently as the applied step changes. For a final comparison , a central slope is
For sufficiently smooth , its leading truncation error is proportional to . Comparing several steps tests that numerical behavior, while choosing steps near the physical reference uncertainty also probes whether a local derivative adequately represents the measurement model.[ref]
For an original model, let and , with . For , the central slopes are0.210,0.2025 and0.200625. Their successive departures from0.2 shrink by four as halves. Richardson extrapolation removes the cubic contribution exactly in this model:
For a general smooth response, it removes the leading term rather than proving exact cancellation of every nonlinear contribution.
Small steps also amplify output error. If each evaluation has absolute error at most , the error in the central slope is at most . With , this bound is at but0.1 at . The cubic truncation term decreases with , whereas this evaluation-error bound increases. Equating their orders, , suggests the scale , here0.001mm. This scale follows from the stipulated error model, not a universal finite-difference setting.
An unchanging central value is also insufficient to establish differentiability. For , every is zero, while the forward and backward slopes are and . Inspecting both one-sided changes reveals the cusp. Likewise, a stable local slope does not rule out a quadratic finite-range response, as finite-perturbation reference sensitivity shows.
A meaningful test changes one assigned shared reference consistently in every dependent calculation, holds the other inputs and computational settings fixed, and records the steps, units, slopes and one-sided changes. Shared reference uncertainty and comparison-process variability are distinct physical contributions in the NIST uncertainty budget.[ref] If evaluation includes simulation noise, separate its repeatability from the response to the changed reference.