David Morris Lee, Douglas Dean Osheroff and Robert Coleman Richardson compressed coexisting liquid and solid helium-3 in a cell precooled by a dilution refrigerator. Helium-4 pressure drove coupled bellows and a piston; a capacitance diaphragm gauge read pressure and platinum nuclear magnetic resonance supplied thermometry. Uniform compression revealed a slope break A and a small pressure drop B; decompression and varied solid fraction checked reproducibility. Their April 1972 paper, Evidence for a New Phase of Solid He3, interpreted a new solid phase, without establishing liquid superfluidity. [ref]
The October follow-up replaced the thermometer assembly with a sample nuclear magnetic resonance coil. An applied magnetic field gradient selected different sample layers, separating strong solid signals from the liquid background. At A the liquid resonance shifted; at B its shift disappeared and its magnetic susceptibility fell. Removing the gradient resolved the frequency shift directly. Independence from solid fraction and distinct relaxation times supported the liquid assignment. Thus the reinterpretation rested on phase-selective evidence, rather than relabeling the first paper's title. These magnetic observations identify changed liquid phases; they do not directly measure frictionless flow. [ref]
Douglas Dean Osheroff recalls the subsequent p-wave interpretation. [ref]
Figure 1.
Compression and independent readout channels in the helium-3 superfluid discovery experiment
. Original functional diagram, not a reconstruction to scale. Left: drive, sample and pressure channel. Right: separate thermometer and sample nuclear magnetic resonance configurations; the latter replaces the former in the follow-up. Connections indicate function, not historical wiring. Details.
The inference has a useful limit. A pressure anomaly in two coexisting phases cannot, by itself, identify which phase changed: both contribute to the common phase coexistence curve. Thermometer lag, a temperature gradient or slow equilibration can also separate indicated temperature from the sample state. Correlating another response with the anomaly provides information that repeating the same pressure trace cannot supply. Conversely, a shifted magnetic resonance alone does not measure a frictionless flow rate.