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In 1962, Riccardo Giacconi and colleagues flew three Geiger counters to search for lunar X-ray fluorescence. Different mica thicknesses tested penetration; lampblack blocked ultraviolet. Each counter sat in an anticoincidence detector using a scintillation counter to reject cosmic rays. There was no mechanical collimator. Rotation scanned the sky; optical sensors supplied orientation.^[ref]

Counts were sorted by azimuth; a faulty counter and tumbling descent data were excluded. A directional peak lay above a diffuse component. Window, altitude and angular responses tested X-rays against charged particles; the Moon's nondetection checked optical leakage. The authors argued for an origin outside the Solar system, while residual cosmic ray background was not directly measured and source size, position and spectrum remained assumption-dependent.^[ref]

A simple original forward problem makes the distinction precise. Let $\varphi$ be the scan azimuth, let $g(\varphi )$ be a dimensionless directional response with maximum one, let $F$ be a source's band-integrated photon arrival rate per unit area, let $A_0$ be its on-axis X-ray effective area, and let $b$ be a constant accepted background rate. The expected rate isFor a broad illustrative response $g(\varphi )=\max (0,\cos \varphi )$, the full width at half maximum is $120^{\circ }$: $\cos \varphi =1/2$ at $\varphi =\pm 60^{\circ }$. For a one-dimensional ideal collimator model $g(\varphi )=\max (0,1-|\varphi |/{\theta }_c)$, the full width at half maximum is ${\theta }_c$. Choosing ${\theta }_c=20^{\circ }$ narrows the response sixfold without focusing any additional photons. These are teaching response functions, not reconstructions of the rocket's window transmission or geometry. A narrower scan peak can reflect the instrument response even when the source is unresolved.

The Geiger-Marsden experiment probes the interior of a chemical atom by counting alpha particles deflected by metal foils. The surprising observation was a small population returning towards the incident side. Hans Geiger and Ernest Marsden performed the experiments under Ernest Rutherford's direction; Ernest Rutherford developed the Rutherford model in 1911. Observation and interpretation were distinct contributions.^[ref]

In 1909, a radon source and its radioactive decay products in a conical glass tube supplied alpha particles through a mica window towards a reflector. Lead shielded a fixed zinc sulfide screen from direct hits; an optical microscope resolved individual particle scintillations. Reflectors occupied the same position. Reflector-out counts tested air scattering; stacked gold foils and bare glass tested thickness and support contributions.^[ref]

Nearby source geometry blurred incidence angles. Extrapolating platinum counts uniformly over a hemisphere was an assumption, not a universal reflection probability.^[ref]

In 1918, Irving Langmuir measured adsorption using freshly split mica strips, handled at their edges, separated by iron spacers and held with brass fasteners. A glass bulb contained the bundle; a similar blank contained matching iron and brass but no mica. Evacuated glass connections, Mercury seals, liquid air traps, and McLeod gauges provided controlled gas handling. Calibrated compartment volumes and pressure readings before and after expansion gave free-gas amounts; their deficit indicated uptake. Lowering pressure and measuring released gas tested desorption.^[ref]

Hydrogen blank runs calibrated cooling-related pressure differences. Irving Langmuir pre-cooled the bulbs to reduce thermal delay; he suggested slow diffusion between strips could control the remaining approach to equilibrium. Critically, blank uptake was not subtracted: he estimated the mica-bulb results were 10–30% too high. Liquid air temperature drift was unrecorded. These limits constrain inference of intrinsic binding from the uptake curve. The paper's pressure unit called “bar” was $1\mathrm{dyn}\mathrm{c}{\mathrm{m}}^{-2}=0.1\mathrm{Pa}$, unlike the modern bar used above.^[ref]