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A measurement method describes the general logical arrangement of operations used to make a measurement. A measurement procedure supplies the detailed instructions for implementing that arrangement with a particular measuring system. The VIM lists substitution measurement methods, null measurement methods, differential methods, and direct or indirect methods among the possible descriptions.^[ref]

For an original substitution measurement method, drive an unknown resistor with a fixed electric current $I$ and record a voltmeter indication. Replace it by an adjustable reference resistor without changing $I$ or the other relevant conditions, and adjust the reference until the indication agrees. In an ideal measurement model,so matching $v_x=v_s$ implies $R_x=R_s$. The common additive readout offset $v_0$ cancels. This cancellation depends on the current, connections and offset remaining common; the name of the method alone does not guarantee those conditions.

A null measurement method instead adjusts a reference to make a difference signal vanish, as in a balanced Wheatstone bridge. A resistance inferred from separately measured electric potential difference and electric current uses the relation $R=V/I$. These are descriptions of how the information is obtained; the operational record must still specify apparatus, settings, timing, reference values and the measurement uncertainty. The measurement principle concerns the physical phenomenon used, while the measurement method concerns the organization of the measurement. Different methods can exploit the same physical principle.

A measurement principle is the phenomenon on which a measurement is based. The VIM gives the thermoelectric effect used to measure temperature as a physical example.^[ref] Naming that phenomenon identifies the physical connection that makes an observable signal informative about the measurand.

A thermocouple uses the Seebeck effect to produce an electric potential difference associated with temperatures along a circuit of dissimilar conductors. In a chosen approximation with constant coefficient $S$, the measurement model can be writtenwhere $T_r$ is the reference-junction temperature. For an original ideal example, choose $S=40\mu \mathrm{V}{\mathrm{K}}^{-1}$, $T_r=20{}^{\circ }\mathrm{C}$ and $V=2.00\mathrm{mV}$. The inferred temperature difference is $50\mathrm{K}$, so $T_h=70{}^{\circ }\mathrm{C}$. These stipulated values illustrate the model, not the calibration of a particular thermocouple type.

The reference condition matters physically: the same signal at $T_r=25{}^{\circ }\mathrm{C}$ would imply $T_h=75{}^{\circ }\mathrm{C}$ in this model. A readout that neglects the reference temperature can give a precise-looking indication without measuring the intended temperature correctly. The measurement principle explains why the signal arises; it does not by itself supply all corrections or the measurement uncertainty.

The measurement method describes how operations are organized around the principle, for example comparing an output with a reference. The measurement procedure specifies the actual conductors, junction arrangement, temperature references, readout settings, settling interval and calculations. Different measuring systems can share a measurement principle while implementing different methods and procedures.

A measurement procedure describes in sufficient detail how a measurement is performed, including its measurement method, measurement model and the calculations that produce a measurement result. The VIM notes that the description usually enables an operator to carry out the measurement and can include a target measurement uncertainty.^[ref] Naming an instrument or writing a final equation alone leaves much of this operational description unspecified.

Consider an original procedure for the resistance measuring system described above. Specify the test resistor and temperature, the two-terminal lead arrangement, source current, readout settings and settling time. Record the measured or assigned current with its measurement uncertainty. First replace the test resistor by a short whose resistance is negligible in the chosen model, and record indication $V_s$. Insert the test resistor without changing the declared lead configuration, allow the specified settling interval and record $V_x$. Repeating the short reading after the sample reading helps check stability.

Assume the current $I$, lead resistance $R_L$ and additive readout offset $V_0$ remain common to the paired readings. Thenso the procedure's calculation isFor stipulated $V_s=3\mathrm{mV}$, $V_x=103\mathrm{mV}$ and $I=1\mathrm{mA}$, this gives $100\Omega$. The paired measurement removes the common lead and zero contributions under the stated model.

The sequence matters because those contributions can change. If the readout offset rises by $0.5\mathrm{mV}$ between the short and sample readings, the same calculation is shifted by $0.5\mathrm{mV}/(1\mathrm{mA})=0.5\Omega$. This is an original instrumental drift example, not observed equipment performance.

Document which operations are repeated, how corrections are obtained, how deviations are handled and which uncertainty contributions remain. The procedure turns the apparatus and model into a repeatable set of operations; it does not make the supplied references, stability assumptions or recorded values exact.

A null measurement method adjusts a reference or a system setting until a difference signal is brought to zero. A null detector tests the residual mismatch; the final measured quantity value follows from the reference and the balance condition. The VIM lists null measurement among measurement methods.^[ref]

A Wheatstone bridge provides a concrete electrical apparatus. The PHYWE manual connects a source across two resistor dividers and a current detector between their middle junctions; balance occurs when those junction potentials agree and detector current vanishes.^[ref] A sliding-wire implementation adjusts the divider ratio continuously.

For an original notation, let the left branch contain upper resistance $R_a$ and lower $R_b$, while the right contains upper unknown $R_x$ and lower reference $R_s$. With source electric potential difference $V_s$ and negligible loading at balance, the middle-junction potentials above the lower supply terminal areSetting $V_L-V_R=0$ yieldsFor $R_a=2000\Omega$, $R_b=1000\Omega$ and $R_s=500\Omega$, the balance identifies $R_x=1000\Omega$ independently of the nonzero source magnitude in this ideal model.

Zero on a display has finite meaning. With $V_s=3\mathrm{V}$, the derivative of residual $V_L-V_R$ with respect to $R_x$ at this balance is $1/1500\mathrm{V}{\mathrm{\Omega }}^{-1}$. A residual magnitude below $10\mu \mathrm{V}$ therefore corresponds locally to about $0.015\Omega$ of unresolved mismatch. A detector zero offset can also shift the apparent balance. The null measurement method reduces reliance on calibrated detector gain at exact balance, but reference uncertainties, lead effects, detector sensitivity and instrumental drift remain relevant to the complete measurement result.

A substitution measurement method compares an unknown with a reference by placing them successively in the same relevant position of a measuring system. The comparison seeks a match or measures a difference while retaining as much of the system response as possible. The VIM lists substitution among measurement methods; the detailed sequence belongs to the measurement procedure.^[ref]

For a physical application, NIST's double substitution weighing procedure compares a standard and an unknown of the same nominal mass twice, using a weighing instrument as a comparator. It also determines response with a known sensitivity mass and includes measurement-assurance checks.^[ref] The measurement standard supplies the reference value; the comparator need not establish the whole mass independently from its own zero.

An original simplified drift model shows why sequence matters. Let a comparator indication at equally spaced time index $t$ bewith fixed response coefficient $a$, additive offset $b$ and linear instrumental drift $d$. Observe standard S at $t=0$, unknown X at $t=1,2$, and S again at $t=3$. The mean X indication and mean S indication have the same mean time $3/2$, givingBoth the constant offset and the stipulated linear drift cancel. For $m_S=m_0=100\mathrm{g}$, $a=500{\mathrm{g}}^{-1}$, $b=10$ and $d=2$, an unknown $m_X=100.004\mathrm{g}$ gives indications $10,14,16,16$. Their paired means differ by two, recovering $0.004\mathrm{g}$.

This teaching sequence isolates one cancellation mechanism; it is not the full NIST procedure. Nonlinear drift, unequal timing, changing response or different positioning can defeat it. NIST's procedure separately addresses buoyancy and uncertainty contributions.^[ref] A close match does not remove the reference's measurement uncertainty or establish that the substitution left every relevant condition unchanged.